A distillation column is a heat engine that instead of work produces a decrease of entropy, i. Dec 16, 2008 with a particular focus on the distillation of highly viscous or selfpolymerized mixtures, this study reports the hydrodynamic and mass transfer performance of two flowguided sieve trays, including their pressure drop, entrainment, weeping and tray efficiency, obtained experimentally with an airwateroxygen system in a. A large amount of performance data on largerscale trays without downcomers has become available recently, and the data have been examined with a view toward understanding and modeling the contacting mechanisms under distillation conditions. The sieve tray distillation column is one of the mo3t widely w,ed sepa. Physical properties data obtained from a typical refinery company, in nigeria for lpg merox unit distillation column is tabulated below. I have a few questions and some clarification would be great. A similar procedurecan be applied in principle to the valve and bubble cap trays, provided critical performance data are available. Distillation sieve tray column how hb hw hap lt column internals sieve plate performance diagram froth ideal. From a capacity viewpoint, a liquid rate greater than 6 gpm inch of weir weir loading, is the rate at which a higher number of flow paths should be considered. Distillation may result in essentially complete separation nearly pure components, or it may be a partial separation that increases the concentration of selected components in the mixture. The graphical solution shows that the example column has a cutpoint of 718.
Reboiler to provide the necessary tray vaporisation the distillation process. From the above, it could be seen that the 8 mm hole flowguided. A weir on the tray ensures that there is always some liquid holdup on the tray and is designed such that the the holdup is at a suitable height, e. Sample calculations involve setting up a process flow diagram of the distillation column, followed. Distillation column designing steps of distillation column.
In figure 1 there is an unlikely case where the enriching section is a tray column and stripping section is a packed column. Find, read and cite all the research you need on researchgate. Eindhoven university of technology master flooding in distillation. It was equipped with a set of 14 sieve trays which have been fabricated of light alloy. Pdf the drawing is based on calculations performed for the dc102 distillation column as part of the design project report. Many people have examined dry tray pressuredrop data for sieve tray decks and there have been several attempts to correlate these data. The column is made of stainless steel material with seven sieve trays. Apply the mccabe thiele graphical design method to determine the number of equilibrium stages in a column describe column internals trays and packing define tray efficiency explain the height of packing equivalent to a theoretical plate thanks to ming thamswebsite for pictures and information. Performance and applications of flowguided sieve trays for. Atmospheric distillation process fundamental concepts. Aeration factor used in estimation of sieve tray pressure drop. Types of tray distillation column a bubble cap tray, b sieve tray. Efficiencies of sieve tray distillation columns by cfd simulation.
Distillation columns are designed to achieve this separation efficiently. The typical gasliquid contacting operations include distillation, absorption. An electrically heated reboiler is installed at the bottom of the column. A bubble cap tray has riser or chimney fitted over each hole, and a cap that covers the riser. Bubble cap trays sieve trays valve trays typically, the liquid flow between trays is governed by a weir on each tray. The sieve tray has been in the distillation market place for many decades. Sieve tray distillation column at best price in india. Distillation principles chemical engineering, 200711, rvce. Feb 04, 2018 operating range bubblecap trays have a positive liquid seal and can therefore operate efficiently at very low vapour rates.
Dual flow tray dual flow tray is a sieve tray without a downcomer. For several column lay outs and different liquid compositions, the hydraulic behaviour on sieve trays as function of liquid and gas flow rates. Pdf sieve trays are widely used in the gasliquid contactors such as distillation and absorption towers. The sieve tray is a perforated plate type tray, with holes punched into the deckplate that typically measure from 316 up through 1 in diameter. Distillation distillation sieve tray column how hb hw hap. The setup is designed to demonstrate principles of distillation in a sieve plate column. Klm technology group practical engineering guidelines for processing plant solutions filename. Sieve trays for viscous mixture distillation applications 1511 korean j.
Vapors move up to the tray above through the hole, while the liquid traveles down in the same hole that can result in maldistribution and low efficiency. Pdf hydrodynamics of sieve tray distillation column. Usa sieve tray distillation column from america manufacturers and exporters usa b2b marketplace providing sieve tray distillation column offers and catalogs from preverified usa suppliers and manufacturers. Column cost is reduced by having fewer trays that are more closely spaced than conventional trays, and the low column pressure drop reduces utility consumption and operating expense.
Fluid velocity larger than ascending bubbles minimum width. This is a perforated sieve tray that employs carefully designed slots to achieve high tray efficiency and extremely low pressure drop. Vapor passes straight upward through the liquid on the plate. Distillation column an overview sciencedirect topics. Valve trays are intended to give greater flexibility than sieve trays at a lower cost. The designed distillation column is a plate tray multicomponent distillation column with a total condenser and a partial reboiler. In this work a cfd simulation is developed to give predictions of the fluid flow patterns, hydraulics, and mass transfer efficiency of distillation sieve trays including a. Feb 25, 2015 7 typesanddesignof the towerstrays mohamedsalah c. The cost of a tray column is determined by two factors. Types and design of the towers trays linkedin slideshare.
The feed to the designed column, which is a mixture of xylenes, aromatics a9, a10, a11 and iparaffin is fed to the 9th plate of the column, from which the desired product is recovered. Pdf study of packed sieve tray column in ethanol purification. Tray operation fundamentals distillation trays generally provide holdup for a portion of liquid through which vapor. Large if froth is expected, also allow space for crawling 12 to 24. A study of entrainment in distillation column for sieve plate. The column is not empty, there are usually either distillation trays or packing in order to increase the contact area between the two phases.
Isnt the weir for plate n1 simply the downcomer for plane n. Theoretical trays calculate the minimum number of theoretical trays with the fenske equation for a better tray count estimate, assume a reflux ratio and run cases in a simulator in aspen plus, use distwu model in hysys, use shortcut column model all column design work is typically done with theoretical trays. In lees loss prevention in the process industries fourth edition, 2012. Hydrodynamics of sieve tray distillation column using cfd simulation article pdf available in chemical and petroleum engineering 492. The sieve tray distillation column consisted of two long sections of glass tube one for the rectifying section and one for the stripping section joined together at the feed plate. Sieve trays rely on the flow of vapours through the holes to hold the liquid on the tray, thus cannot operate at very low vapour rates. Column tray and packing design university of oklahoma. Distillation is a process by which two compounds are separated due to differences in their physical properties. Distillation is the process of separating the components or substances from a liquid mixture by using selective boiling and condensation. Pdf hydrodynamics of sieve tray distillation column using. The purpose of the distillation tray efficiency at total reflux experiment is to determine the dependence of the murphree tray efficiency on the vapor flow rate for a bubble cap and for a sieve tray. It has been used extensively in distillation columns worldwide as a highly efficient vaporliquidcontacting device.
Engineering design guidelines distillation column rev 03 web. The numbers of flowpaths of liquid on tray are 1, 2, 3 or 4 as per liquid capacity requirement of column. Fouling tendency allowable pressure drop turndown requirements use kisters table or consult vendor column zoning can help capacity ref h. Table 1 physical properties data for crude oil lpg merox unit key dimensions of the tray column column cross section, m2 5. Being lighter, vapour flows up the column and is forced to pass through the liquid, via the openings on each tray. Feb 25, 2016 im reading mccabe and thieles classic unit operations of chemical engineering section about the design of sieve plate columns. Determine appropriate tray or packing type based on application consider. Pdf efficiencies of sieve tray distillation columns by. Pdf sieve tray becomes a popular contacting device in distillation process because of its relative simplicity and low cost. Trays are widely used in distillation columns because they are easy to. Structured packing, valve trays, bubble cap trays, sieve trays. Vapor comes out of the holes which in turn, keeps the liquid from weeping through.
Usa sieve tray distillation column,sieve tray distillation. View notes distillation from petroleum 402 at pandit deendayal petroleum university. As an example, table 3 shows yields for a crude unit. Figure 1 shows the total distillate percentage on the crude tbp curve. A sieve plate distillation column is separating a feed that is 50mol% nhexane and 50mol% nheptane. Irreversibility analysis of a separation system using sieve. Pdf hydrodynamics of sieve tray distillation column using cfd.
580 1422 487 1309 1075 217 317 934 1367 856 1176 1556 147 79 845 701 1140 503 363 990 1427 1339 1269 648 1074 486 1318 226 750 1517 603 527 1117 16 556 220 1432 893 1183 496 998 402 887